佛山科学技术学院学报(自然科学版)2025,Vol.43Issue(3):76-83,8.
磁性催化剂Co-Fe3O4/α-FeOOH的制备与表征
Synthesis and characterization of magnetic catalyst Co-Fe3O4/α-FeOOH
摘要
Abstract
In order to obtain a catalyst with high performance,simple preparation and easy recovery,a magnetic composite catalyst Co-Fe3O4/α-FeOOH was synthesized by one-step atmospheric aging method.Trimethoprim(TMP)was used as the target pollutant.According to the removal effect of TMP by advanced oxidation system,the optimum preparation conditions of the material were determined.The results show that the optimum preparation parameters of Co-Fe3O4/α-FeOOH catalyst are as follows:Co2+doping ratio is 3%,aging temperature is 100℃ and reaction time is 8 h.Based on the characterization analysis of composition and morphology,the material is composed of rod-like α-FeOOH and granular Fe3O4 with mesoporous structure.The average pore size is 11.59 nm and the specific surface area is 54.64 m2/g.It has good crystallinity and high purity,and the three elements of Fe,Co and O are evenly distributed.The saturation magnetization of the material is 14.45 emu/g.关键词
Co-Fe3O4/α-FeOOH/磁性催化剂/常压老化/甲氧苄啶Key words
Co-Fe3O4/α-FeOOH/magnetism catalyst/atmospheric aging method/trimethoprim分类
资源环境引用本文复制引用
洪俊贤,许俊鸽,张景杭..磁性催化剂Co-Fe3O4/α-FeOOH的制备与表征[J].佛山科学技术学院学报(自然科学版),2025,43(3):76-83,8.基金项目
福建省中青年教师教育科研重点项目(JZ240096) (JZ240096)
黎明职业大学2023年度规划项目资助(LZ202310) (LZ202310)
黎明职业大学博士科研启动基金资助(LZB202301) (LZB202301)