华东师范大学学报(自然科学版)Issue(4):124-133,10.DOI:10.3969/j.issn.1000-5641.2025.04.013
差示扫描量热法在蜂蜜掺假鉴别中的应用
Application of Differential Scanning Calorimetry in honey adulteration
摘要
Abstract
This study explored the feasibility of applying Differential Scanning Calorimetry(DSC)to identify adulteration in five honey samples from Qinghai and neighboring regions.Adulterated samples with adulteration levels(syrup mass/honey mass)ranging from 0,0.05,0.1,0.15,…,to 0.95 were prepared using fructose-glucose syrup or maltose syrup as adulterants.DSC curves were generated to analyze the relationship between DSC signals and temperature.SPSSPRO software was used for modeling,employing a stepwise regression method to establish models for the glass transition onset(Tg0)and midpoint(Tgm).Significance analysis revealed the following:for nitraria honey adulterated with fructose-glucose syrup,the significance level exceeded 0.05.When adulterated with maltose syrup,the Tgm during the cooling phase showed a significance level>0.05.For goji berry honey adulterated with fructose-glucose syrup,Tgm in the cooling phase was also a key parameter.For other samples,Tg0 and Tgm during the heating phase demonstrated strong significance.These results indicate that combining DSC data with modeling methods is efficient and accurate for honey adulteration identification.However,no consistent patterns were observed among different honey types.关键词
蜂蜜掺假鉴别/差示扫描量热法/果葡糖浆/麦芽糖浆Key words
identification of honey adulteration/Differential Scanning Calorimetry(DSC)/fructose syrup/maltose syrup分类
化学化工引用本文复制引用
柴明霞,吕梦瑶,张明潮..差示扫描量热法在蜂蜜掺假鉴别中的应用[J].华东师范大学学报(自然科学版),2025,(4):124-133,10.基金项目
青海大学实验教育教学项目(SYJG202209) (SYJG202209)