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差示扫描量热法在蜂蜜掺假鉴别中的应用

柴明霞 吕梦瑶 张明潮

华东师范大学学报(自然科学版)Issue(4):124-133,10.
华东师范大学学报(自然科学版)Issue(4):124-133,10.DOI:10.3969/j.issn.1000-5641.2025.04.013

差示扫描量热法在蜂蜜掺假鉴别中的应用

Application of Differential Scanning Calorimetry in honey adulteration

柴明霞 1吕梦瑶 2张明潮1

作者信息

  • 1. 青海大学 省部共建三江源生态与高原农牧业国家重点实验室,西宁 810016
  • 2. 青海大学 化工学院,西宁 810016
  • 折叠

摘要

Abstract

This study explored the feasibility of applying Differential Scanning Calorimetry(DSC)to identify adulteration in five honey samples from Qinghai and neighboring regions.Adulterated samples with adulteration levels(syrup mass/honey mass)ranging from 0,0.05,0.1,0.15,…,to 0.95 were prepared using fructose-glucose syrup or maltose syrup as adulterants.DSC curves were generated to analyze the relationship between DSC signals and temperature.SPSSPRO software was used for modeling,employing a stepwise regression method to establish models for the glass transition onset(Tg0)and midpoint(Tgm).Significance analysis revealed the following:for nitraria honey adulterated with fructose-glucose syrup,the significance level exceeded 0.05.When adulterated with maltose syrup,the Tgm during the cooling phase showed a significance level>0.05.For goji berry honey adulterated with fructose-glucose syrup,Tgm in the cooling phase was also a key parameter.For other samples,Tg0 and Tgm during the heating phase demonstrated strong significance.These results indicate that combining DSC data with modeling methods is efficient and accurate for honey adulteration identification.However,no consistent patterns were observed among different honey types.

关键词

蜂蜜掺假鉴别/差示扫描量热法/果葡糖浆/麦芽糖浆

Key words

identification of honey adulteration/Differential Scanning Calorimetry(DSC)/fructose syrup/maltose syrup

分类

化学化工

引用本文复制引用

柴明霞,吕梦瑶,张明潮..差示扫描量热法在蜂蜜掺假鉴别中的应用[J].华东师范大学学报(自然科学版),2025,(4):124-133,10.

基金项目

青海大学实验教育教学项目(SYJG202209) (SYJG202209)

华东师范大学学报(自然科学版)

OA北大核心

1000-5641

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