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25%联苯·噻虫胺微乳剂高效液相色谱分析

梁观凤 侯影 曹俊丽

农药科学与管理2025,Vol.46Issue(7):37-43,7.
农药科学与管理2025,Vol.46Issue(7):37-43,7.

25%联苯·噻虫胺微乳剂高效液相色谱分析

Method Development for the Determination of Bifenthrin+Clothianidin 25%ME

梁观凤 1侯影 1曹俊丽2

作者信息

  • 1. 上海悦联生物科技有限公司,上海 201512
  • 2. 上海悦联化工有限公司,上海 201512
  • 折叠

摘要

Abstract

In this paper,a simultaneous analytical method was established for determining of bifenthrin and clothianidin in a 25%micro-emulsions(ME).High-performance liquid chromatography(HPLC)with a diode-array detector(DAD)set at 230 nm was employed.The separation was achieved using a stainless steel column filled with C18/5 μm,with acetonitrile and an phosphoric acid aqueous solution as the mobile phase.The results showed that correlation coefficients(R2)of 1.000 0 for both active ingredients,the standard deviation of 0.102 6%and 0.065 6%,the variation coefficient of 0.687 5%and 0.660 4%,the average recovery of 100.19%and 99.90%were obtained for bifenthrin and clothianidin,respectively.

关键词

联苯菊酯/噻虫胺/高效液相色谱

Key words

bifenthrin/clothianidin/HPLC

分类

农业科技

引用本文复制引用

梁观凤,侯影,曹俊丽..25%联苯·噻虫胺微乳剂高效液相色谱分析[J].农药科学与管理,2025,46(7):37-43,7.

农药科学与管理

1002-5480

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