矿产综合利用2025,Vol.46Issue(3):10-17,8.DOI:10.12476/kczhly.202208260543
蛭石@淀粉碳化物复合材料的制备及优化
Preparation and Optimization of Vermiculite@Starch Carbide Composites
摘要
Abstract
Vermiculite@starch carbide composites were prepared by hydrothermal carbonization of vermiculite and starch.The prepared composites were washed alternately with deionized water and absolute ethanol.The results of scanning electron microscopy(SEM)and infrared spectroscopy(FTIR)showed that starch carbide was successfully loaded on the surface of vermiculite.The preparation process of the composite was optimized by single factor and response surface method based on the phenol adsorbability index of the composite,and the optimal preparation process parameters were obtained as follows:The mass ratio of starch to vermiculite was 2.97∶1,the carbonization time was 15.66 h,and the carbonization temperature was 196.47℃.At these conditions,the composite material has the best adsorption performance for phenol,and its adsorption capacity for phenol is 16.521 mg/g,which is 4.304 mg/g higher than that of natural vermiculite.关键词
蛭石/淀粉/复合材料/制备工艺优化Key words
vermiculite/starch/composite material/optimization of preparation process分类
矿业与冶金引用本文复制引用
杜慧聪,韦开放,黄晶晶,刘云鹤,王伟,蓝平,蓝丽红..蛭石@淀粉碳化物复合材料的制备及优化[J].矿产综合利用,2025,46(3):10-17,8.基金项目
国家自然科学基金项目(51464006) (51464006)
国家级大学生创新训练项目(202010608011) (202010608011)