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连续流动注射分光光度法测定水中总氰化物实验条件研究

姜军委 王平东

新疆环境保护2025,Vol.47Issue(2):49-56,8.
新疆环境保护2025,Vol.47Issue(2):49-56,8.

连续流动注射分光光度法测定水中总氰化物实验条件研究

Study on Experimental Conditions for Determination of Total Cyanide in Water by Continuous Flow Injection Spectrophotometry

姜军委 1王平东2

作者信息

  • 1. 昌吉生态环境监测站 新疆 昌吉 831100
  • 2. 昌吉州检验检测中心 新疆 昌吉 831100
  • 折叠

摘要

Abstract

Cyanide is a highly toxic substance which is widely present in nature and can enter the body through various pathways to endanger human health.As a standard method for the determination of cyanide in water,spectrophotometry has complicated operation steps and high probability of errors.Compared with traditional spectrophotometry,continuous flow injection analysis is simple and accurate.In order to accurately determine the concentrations of total cyanide in water.,the optimal experimental conditions for the determination of total cyanide in water by continuous flow injection analyzer were determined by control variable method,in which citric acid was used as the distillation reagent,with potassium hydrogen phthalate as the buffer solution,and the pH value of the chromogenic agent was adjusted to 5.2,where Chloramine-T solution must be prepared fresh immediately before use.Consequently,This optimized methodology significantly enhanced water quality analysis efficiency,reduced reagent consumption,and improved both detection sensitivity and accuracy.

关键词

总氰化物/连续流动注射分析/分光光度法/控制变量法

Key words

total cyanide/continuous flow analysis/spectrophotometry/controlled variable method

分类

资源环境

引用本文复制引用

姜军委,王平东..连续流动注射分光光度法测定水中总氰化物实验条件研究[J].新疆环境保护,2025,47(2):49-56,8.

新疆环境保护

1008-2301

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