湿法冶金2025,Vol.44Issue(5):681-691,11.DOI:10.13355/j.cnki.sfyj.2025.05.014
基于响应曲面法的铜电解废液脱杂工艺参数优化研究
Optimization of Process Parameters for Impurity Removal of Copper Electrolysis Waste Liquid Based on Response Surface Methodology
吕喜聪 1唐文涛 2梁柱俊 2刘远东 2李梦雪3
作者信息
- 1. 贵溪冶炼厂冶金化工研究所,江西贵溪 335424||江西铜业集团(贵溪)冶化新技术有限公司,江西贵溪 335424
- 2. 贵溪冶炼厂冶金化工研究所,江西贵溪 335424
- 3. 江西铜业技术研究院有限公司,江西南昌 330096
- 折叠
摘要
Abstract
Removal of impurities(arsenic,antimony,bismuth)from copper electrolytic waste liquid by hydrogen sulfide was studied.The effects of the excess coefficient of hydrogen sulfide,reaction temperature,reaction time and stirring speed on the impurity removal of copper electrolytic waste liquid were investigated.The experimental conditions were further optimized by the response surface methodology,and the experiments were verified under these conditions.The results show that the optimal test conditions are as follows:the excess coefficient of hydrogen sulfide is 1.9,the reaction temperature is 68.1℃,the reaction time is 2.1 h,and the stirring speed is 524 r/min.Under the optimal conditions,the average impurity removal rate of copper electrolysis waste liquid can reach 94.2%.The optimized process parameters determined by the method are reliable and applicable,and will not affect the subsequent recovery of nickel elements.关键词
铜电解废液/响应面法/硫化氢/除杂/砷/锑/铋Key words
copper electrolysis waste liquid/response surface methodology/hydrogen sulfide/impurity removal/arsenic/antimony/bismuth分类
矿业与冶金引用本文复制引用
吕喜聪,唐文涛,梁柱俊,刘远东,李梦雪..基于响应曲面法的铜电解废液脱杂工艺参数优化研究[J].湿法冶金,2025,44(5):681-691,11.