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二步还原温度对铼粉物理性能的影响

LI Xiongbin LIU Xiaoqing XI Yaoyao LI Songbin

铜业工程Issue(6):29-35,7.
铜业工程Issue(6):29-35,7.DOI:10.3969/j.issn.1009-3842.2025.06.004

二步还原温度对铼粉物理性能的影响

Optimization of Two-Step Reduction Temperature on Physical Properties of Rhenium Powders

LI Xiongbin 1LIU Xiaoqing 1XI Yaoyao 1LI Songbin1

作者信息

  • 1. Jiangxi Copper Technology Institute Co.,Ltd.,Nanchang 330096,China||Jiangxi Copper Corporation Limited,Nanchang 330096,China||Jiangxi Provincial Key Laboratory of Rare and Scattered Metals Materials,Jiangxi Copper Corporation Limited,Nanchang 330096,China
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摘要

Abstract

Rhenium powder is an important doping raw material in the aerospace and nuclear industries.Its exceptional physical properties are prerequisite for its application.This study utilized high-purity ammonium rhenate from Guixi Smelter of Jiangxi Copper Corporation Limited as raw material,and devised a gradient of six two-step reduction temperatures.By employing equipment such as field emission scanning electron microscopy(FESEM),powder comprehensive characteristic analyzer,laser particle size analyzer,Fisher particle size analyzer,and oxygen-nitrogen-hydrogen analyzer,we comprehensively assessed the effects of reduction temperatures on the physical properties of rhenium powders.The research results indicated that when the two-step reduction temperature fell within the range of 800℃to 900℃,rhenium powder exhibited superior physical properties,achieving a compact density over 10 g/cm3.Besides,the oxygen content satisfied the specifications stipulated in the superior Re standard of YS/T 1017-2015.

关键词

铼粉/氢还原/还原温度/物理性能/氧含量

Key words

rhenium powder/hydrogen reduction/reduction temperature/physical property/oxygen content

分类

矿业与冶金

引用本文复制引用

LI Xiongbin,LIU Xiaoqing,XI Yaoyao,LI Songbin..二步还原温度对铼粉物理性能的影响[J].铜业工程,2025,(6):29-35,7.

基金项目

赣鄱俊才支持计划·主要学科学术和技术带头人培养项目(20243BCE51179)资助 (20243BCE51179)

铜业工程

1009-3842

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