中国现代中药2025，Vol.27Issue(12)：2288-2295,中插7-中插9,11.DOI:10.13313/j.issn.1673-4890.20241030003
基于近红外光谱的枸橘质量快速评价
Rapid Quality Evaluation of Medicinal Materials Derived from Citrus trifoliata Fruit Based on Near-infrared Spectroscopy
摘要
Abstract
Objective:To establish qualitative and quantitative near-infrared spectroscopy(NIRS)-based models for the medicinal materials derived from Citrus trifoliata fruit to enable rapid quality evaluation.Methods:A total of 100 batches of medicinal materials derived from C.trifoliata fruit were collected.Discriminant analysis was employed to develop a qualitative model distinguishing between yellow and green samples.The content of five bioactive compounds(narirutin,naringin,poncirin,imperatorin,and auraptene)in the 100 batches of samples was determined by high-performance liquid chromatography(HPLC).Partial least squares regression(PLSR)was then employed to construct quantitative calibration models for these components.Results:The qualitative model successfully classified C.trifoliata fruit samples into yellow and green categories,with validation confirming reliable color-based differentiation.Quantitative models for all the five compounds demonstrated good predictive performance,with mean relative errors of 0.083,0.093,0.041,0.197,and 0.143,respectively.Conclusion:The established NIRS-based qualitative and quantitative models proved stable and reliable,facilitating rapid quality evaluation of medicinal materials derived from C.trifoliata fruit.关键词
枸橘/近红外光谱/定性分析/定量分析Key words
Citrus trifoliata fruit/near-infrared spectroscopy/qualitative analysis/quantitative analysis分类
医药卫生引用本文复制引用
ZHANG Shangge,LAN Jinxu,CHEN Pei,CHEN Suiqing,ZHANG Yundian..基于近红外光谱的枸橘质量快速评价[J].中国现代中药,2025,27(12):2288-2295,中插7-中插9,11.基金项目
河南省中医药科学研究专项(2022ZY1174) （2022ZY1174）
河南省中药材产业技术体系项目(豫财科[2023]14号) （豫财科[2023]14号）
