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棕榈叶纤维素纳米晶体的制备与表征

邓新成 张金超 陈卓 胡志军 吴朝军 张诚 沈静

中国造纸2026,Vol.45Issue(1):12-19,8.
中国造纸2026,Vol.45Issue(1):12-19,8.DOI:10.11980/j.issn.0254-508X.2026.01.002

棕榈叶纤维素纳米晶体的制备与表征

Extraction and Characterization of Cellulose Nanocrystal from Palm Leaves(Trachycarpus Fortunei)

邓新成 1张金超 2陈卓 1胡志军 1吴朝军 3张诚 4沈静5

作者信息

  • 1. 浙江科技大学环境与资源学院,浙江 杭州,310023
  • 2. 浙江科技大学环境与资源学院,浙江 杭州,310023||东北林业大学材料科学与工程学院,黑龙江 哈尔滨,150040||齐鲁工业大学(山东省科学院)制浆造纸科学与技术教育部重点实验室,山东 济南,250353||仙鹤股份有限公司,浙江 衢州,324022
  • 3. 齐鲁工业大学(山东省科学院)制浆造纸科学与技术教育部重点实验室,山东 济南,250353
  • 4. 仙鹤股份有限公司,浙江 衢州,324022
  • 5. 东北林业大学材料科学与工程学院,黑龙江 哈尔滨,150040
  • 折叠

摘要

Abstract

In this study,palm leaves were utilized as raw materials to prepare cellulose nanocrystal(CNC)through a combination of chemical treatment and acid hydrolysis,followed by analysis and characterization.Firstly,cellulose fibers were extracted from palm leaves via sodium chlorite treatment and alkaline treatment.Subsequently,the extracted cellulose fibers were hydrolyzed using concentrated sulfuric acid to pro-duce CNC.The microscopic morphology and chemical composition of the palm leaf fibers were characterized using Fourier transform infrared spectroscopy(FT-IR),X-ray diffraction(XRD),thermogravimetric analysis(TG),scanning electron microscopy(SEM),and transmission elec-tron microscopy(TEM).The results showed that non-cellulosic components(lignin and hemicellulose)in the palm leaves were successfully re-moved through chemical treatment.After acid hydrolysis,rod-shaped CNC were successfully isolated.The yield of cellulose fibers from palm leaves reached 23.1%.The extracted CNC exhibited a crystallinity of 75%and an average aspect ratio of 18.

关键词

棕榈叶/纤维素纳米晶体/脱木质素/酸水解

Key words

palm leaves/cellulose nanocrystal/delignification/acid hydrolysis

分类

轻工纺织

引用本文复制引用

邓新成,张金超,陈卓,胡志军,吴朝军,张诚,沈静..棕榈叶纤维素纳米晶体的制备与表征[J].中国造纸,2026,45(1):12-19,8.

基金项目

浙江科技大学环境与资源学院青年教师创新研究项目(HZQY202414) (HZQY202414)

制浆造纸科学与技术教育部重点实验室开放基金项目(KF202309) (KF202309)

浙江科技大学基本科研业务费专项资金项目(2025QN058). (2025QN058)

中国造纸

0254-508X

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