高等学校化学学报2026，Vol.47Issue(2)：18-26,9.DOI:10.7503/cjcu20250208
不同形貌氧化锌微米晶体的水热法控制合成
Controlled Synthesis of Zinc Oxide Microcrystals with Distinct Morphologies via Hydrothermal Method
摘要
Abstract
A method of hydrothermal synthesis coupled with activation etching was employed to synthesize zinc oxide(ZnO)particles with six distinct morphologies:rod,tube,screw,rod-flower,tube-flower,and screw-flower.The controlled synthesis of ZnO from dispersed rods to aggregated rod-flower clusters was achieved by adjusting the parameters of the hydrothermal reaction.Moreover,by exploiting the differences in the stability of various crystal faces,a customized post-etching method was used to effectively control the morphological evolution of ZnO from rod-like structure to tubular and screw-like structures.The results of photoelectrochemical test indicated that the distinct morphology of ZnO played a significant role in its photoelectrochemical property.These findings offer valuable insights into the synthesis of ZnO with specific morphologies to tailor its properties for particular application.关键词
氧化锌/晶体形貌/控制合成/光电化学性质Key words
Zinc oxide/Crystal morphology/Controlled synthesis/Photoelectrochemical property分类
化学化工引用本文复制引用
陈杨,王芙香,仇一朵,黄宇桐,赵晓君,潘勤鹤..不同形貌氧化锌微米晶体的水热法控制合成[J].高等学校化学学报,2026,47(2):18-26,9.基金项目
国家自然科学基金(批准号:22461016,22361017)、海南省自然科学基金(批准号:524MS027)和海南省院士创新平台科研项目(批准号:YSPTZX202321)资助. Supported by the National Natural Science Foundation of China(Nos.22461016,22361017),the Hainan Provincial Natural Science Foundation,China(No.524MS027)and the Specific Research Fund of the Innovation Platform for Academicians of Hainan Province,China(No.YSPTZX202321). （批准号:22461016,22361017）
