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基于空气动力学透镜的在线热解吸进样系统的研制与初步测试

陈漫琪 卓泽铭 郑义炯 张国华 李梅 李雪 李磊

分析测试学报2026,Vol.45Issue(2):420-427,8.
分析测试学报2026,Vol.45Issue(2):420-427,8.DOI:10.12452/j.fxcsxb.25070501

基于空气动力学透镜的在线热解吸进样系统的研制与初步测试

Development and Preliminary Testing of an Online Thermodesorption Sampling System Based on Aerodynamic Lens

陈漫琪 1卓泽铭 2郑义炯 3张国华 4李梅 1李雪 1李磊1

作者信息

  • 1. 暨南大学 环境与气候学院,广东 广州 510632
  • 2. 威凯检测技术有限公司,广东 广州 510700||中国电器科学研究院股份有限公司,广东 广州 510000
  • 3. 广东省麦思科学仪器创新研究院,广东 广州 510700
  • 4. 中国科学院广州地球化学研究所,广东 广州 510640
  • 折叠

摘要

Abstract

This study developed an online aerosol thermodesorption sampling system based on an aerodynamic lens.The system primarily consists of a gas-phase denuder,a high-throughput wide-range lens,and a thermodesorption module.The lens sampling system,optimized through fluid sim-ulation,achieves high-flow sampling at 575 mL/min and a wide particle transmission range of 0.1-13.0 μm.Experimental results demonstrate that the gas-phase denuder achieves 99.74%adsorption efficiency for volatile gases and maintains particle transmission efficiency ranging from 93.56%to 99.70%for particles within the 100-500 nm size range,effectively eliminating VOCs interference in organic aerosol samples while minimizing particle transmission losses.The lens thermodesorption sampling system was coupled with a single photon ionization time of flight mass spectrometer(SPI-MS)to conduct online detection and analysis of smoke particles from different biomass combustion sources,including cigarettes,moxa sticks,and mosquito coils.This work demonstrates the appli-cation capability of this combined system for detecting particle-phase VOCs of biomass combustion products.The aerosol sampling system can be used for a variety of traditional vacuum-ionization mass spectrometers,and has a broad application prospect.

关键词

气溶胶/挥发性有机物/空气动力学透镜/真空电离源质谱仪

Key words

aerosol/volatile organic compounds/aerodynamic lens/vacuum ionization source mass spectrometer

分类

化学化工

引用本文复制引用

陈漫琪,卓泽铭,郑义炯,张国华,李梅,李雪,李磊..基于空气动力学透镜的在线热解吸进样系统的研制与初步测试[J].分析测试学报,2026,45(2):420-427,8.

基金项目

国家重点研发计划青年科学家项目(2022YFF0705400) (2022YFF0705400)

暨南大学科协青年科技人才托举工程项目(21623205) (21623205)

分析测试学报

1004-4957

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