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氧化钇添加量对牙科氧化锆陶瓷光学性能的影响

何林峰 刘飞 沈颉飞

国际口腔医学杂志2026,Vol.53Issue(2):197-204,8.
国际口腔医学杂志2026,Vol.53Issue(2):197-204,8.DOI:10.7518/gjkq.2026217

氧化钇添加量对牙科氧化锆陶瓷光学性能的影响

Effect of yttria doping content on the optical properties of dental zirconia

何林峰 1刘飞 1沈颉飞1

作者信息

  • 1. 口腔疾病防治全国重点实验室 国家口腔医学中心 口腔疾病国家临床医学研究中心四川大学华西口腔医院修复Ⅱ科 成都 610041
  • 折叠

摘要

Abstract

Objective This study aims to investigate the effect of yttria doping content on the microstructural changes and optical properties of zirconia. Methods Zirconia materials from the same brand,with yttria additions of 3 mol%(3Y),4 mol% (4Y),and 5 mol% (5Y),were employed. Presintered discs were prepared,and sample specifications were designed,cut,and densified accordingly. For microstructural characterization,ceramic samples were sintered into circular discs with a diameter of 9 mm and a thickness of 2 mm. For optical performance characterization,ceramic samples were sintered into square plates measuring 6 mm× 8 mm,with thicknesses ranging from 0.5-1.0 mm in equal intervals. A total of 6 groups (n=5) were prepared. Surface morphology was examined using scanning electron microscopy,and the crystal phase proportion was refined via X-ray diffraction. The refractive index was measured with an ellipsometer,and transmittance and the contrast ratio (CR) were evaluated using a spectrophotometer. Results Increasing the yt-tria doping level resulted in enlarged crystal diameters.Among the groups,4Y exhibited the largest tetragonal phase proportion (59.49%),and 5Y had the smallest (19.46%). The refractive index decreased with increased yttria doping. Transmittance was substantially influenced by wavelength and material thickness,with long wavelengths (705 nm) achieving the highest transmittance and short wavelengths(435 nm) having the lowest for all materials. The transmittance values of the 3Y and 4Y groups were below 1%. The trans-mittance of the 5Y group exceeded 10% at long wavelengths (705 nm) and was below 1% at short wavelengths (435 nm).The CR values were minimally affected by thickness. The 3Y and 4Y groups had average CR values of 0.8±0.1,and statis-tical differences were observed only between select groups. The 5Y group had an average CR value of 0.4±0.2,which was statistically significantly different from those of the other groups. Conclusion Low yttria doping levels promoted the growth of tetragonal-phase crystals,and high yttria levels significantly enhanced the formation of cubic-phase crystals. A doping level of 5 mol% yttria is necessary to effectively improve the translucency of zirconia.

关键词

氧化锆/氧化钇/四方相/立方相/光学性能/折射率/半透性

Key words

zirconia/yttria/tetragonal phase/cubic phase/optical property/refractive index/translucency

分类

医药卫生

引用本文复制引用

何林峰,刘飞,沈颉飞..氧化钇添加量对牙科氧化锆陶瓷光学性能的影响[J].国际口腔医学杂志,2026,53(2):197-204,8.

基金项目

National Key Research and Development Program of China(2022YFC2410102) 国家重点研发计划(2022YFC2410102) (2022YFC2410102)

国际口腔医学杂志

1673-5749

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