佛山科学技术学院学报(自然科学版)2026,Vol.44Issue(2):79-85,7.
基于表面增强拉曼光谱快速检测面粉中的脱氢乙酸钠
The rapid detection of sodium dehydroacetate in flour by Surface-enhanced Raman spectroscopy
卢昆达1
作者信息
- 1. 佛山大学食品科学与工程学院,广东 佛山 528225
- 折叠
摘要
Abstract
In order to study the Raman spectrum of sodium dehydroacetate and the vibrational mode between its molecular chemical bonds,the density functional theory was used to calculate and analyze the Raman spectrum peaks.The preparation conditions of silver sol were optimized by different dosages of sodium citrate and different heating durations.Additionally,the surface-enhanced Raman shift of sodium dehydroacetate in flour was qualitatively studied.Detection results showed that the solid standard of sodium dehydroacetate had obvious Raman characteristic peaks at 358,631,1 260,1 404,1 660,2 928 cm-1.By optimizing the preparation conditions of silver sol,the minimum detection limit of sodium dehydroacetate in flour was 0.1%.The enhanced Raman spectra of sodium dehydroacetate spiked in flour were pretreated and combined with stoichiometry to establish the best partial least squares model which realized the rapid detection of sodium dehydroacetate in flour.关键词
表面增强拉曼光谱/密度泛函理论/脱氢乙酸钠Key words
Surface-enhanced Raman spectroscopy/density functional theory/sodium dehydroacetate分类
轻工纺织引用本文复制引用
卢昆达..基于表面增强拉曼光谱快速检测面粉中的脱氢乙酸钠[J].佛山科学技术学院学报(自然科学版),2026,44(2):79-85,7.