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煤化工污泥中水分赋存状态分析方法研究

柳金秋 李泰山 孙海勇 何国锋 刘烨炜 李磊 程子睿

煤质技术2026,Vol.41Issue(2):54-59,6.
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煤质技术2026,Vol.41Issue(2):54-59,6.DOI:10.3969/j.issn.1007-7677.2026.02.07

煤化工污泥中水分赋存状态分析方法研究

Research on the analysis method of moisture storage state in coal chemical sludge

柳金秋 1李泰山 2孙海勇 1何国锋 1刘烨炜 1李磊 1程子睿3

作者信息

  • 1. 中煤科工清洁能源股份有限公司,北京 100013
  • 2. 内蒙古伊泰化工有限责任公司,内蒙古 鄂尔多斯 017400
  • 3. 南京理工大学物理学院,江苏 南京 210094
  • 折叠

摘要

Abstract

Coal chemical sludge has high moisture content,high viscosity,and contains toxic and harmful substances.Its reduction and harmless disposal have become a challenge for the green and sustainable development of the chemical industry.In order to reveal the occurrence status of water in sludge and lay the research foundation for sludge disposal,differential scanning calorimetry(DSC)and low field nuclear magnetic resonance(NMR)methods were used to analyze the water forms in sludge.The results indicate that DSC method cannot accurately analyze the occurrence status of water in sludge.By using NMR testing method,the water in sludge can be divided into four types:intracellular water,ad⁃sorbed water,interstitial water,and free water.The analysis results show that the intracellular water content in chemi⁃cal sludge is 1.43%to 6.83%,adsorbed water content is 2.95%to 63.09%,interstitial water content is 31.04%to 94.23%,and free water content is 0 to 1.03%,distinguishing the water content in different states of sludge has impor⁃tant guiding significance for the study of water removal or bound water conversion in sludge.

关键词

煤化工污泥/减量化/水分状态测定/差示扫描量热仪/低场核磁

Key words

chemical sludge/reduction/moisture state analysis/differential scanning calorimeter/low field nu⁃clear magnetic resonance

分类

资源环境

引用本文复制引用

柳金秋,李泰山,孙海勇,何国锋,刘烨炜,李磊,程子睿..煤化工污泥中水分赋存状态分析方法研究[J].煤质技术,2026,41(2):54-59,6.

基金项目

中国煤炭科工集团有限公司科技创新创业资金专项资助项目(2024-ZD005) (2024-ZD005)

煤质技术

1007-7677

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