中国中药杂志2026,Vol.51Issue(6):1565-1572,8.DOI:10.19540/j.cnki.cjcmm.20251028.301
抗氧化剂在肉桂挥发油包合物喷雾干燥中的保护作用研究
Protective effect of antioxidants in spray drying of cinnamon essential oil inclusion complexes
摘要
Abstract
Spray drying is widely employed in the preparation of essential oil inclusion complexes.However,due to the high-temperature environment during drying,this technology often results in oxidative loss of essential oils within these inclusion complexes.To address this issue,this study utilized the inclusion complexes prepared from cinnamon essential oil and measured thiobarbituric acid reactive substances(TBARS)value and peroxide value(POV).Among the six antioxidants such as octyl gallate,L-ascorbyl palmitate,and propyl gallate,the antioxidants that could significantly enhance the retention rate of volatile components in the spray drying process of essential oil inclusion complexes were screened out and used as"protective agents"during the spray drying process.Furthermore,by combining a 15-day high-temperature stability test with GC-MS analysis,the effects of varying antioxidant concentrations on the retention rate of volatile components,high temperature stability,and their components in the inclusion complexes were investigated.The results revealed that both octyl gallate and propyl gallate demonstrated considerable potential in effectively preserving the volatile components.In addition,these antioxidants at specific concentrations markedly reduced the loss of volatile components and enhanced the protecting effect.The retention rates of volatile components reached 90.38%and 87.96%for octyl gallate and propyl gallate,respectively,compared to 78.36%in the control group.The protective effect was particularly pronounced at an antioxidant concentration of 0.04%under the high-temperature stability test.GC-MS analysis confirmed that the incorporation of antioxidants did not interfere with the chemical composition of the essential oil.Therefore,the addition of appropriate concentrations of antioxidants during the preparation of essential oil inclusion complexes can effectively mitigate oxidative loss and improve both the retention and stability of volatile components.关键词
抗氧化剂/没食子酸辛酯/没食子酸丙酯/挥发油稳定性/包合物/喷雾干燥Key words
antioxidant/octyl gallate/propyl gallate/essential oil stability/inclusion complex/spray drying引用本文复制引用
胡恢权,万娜,刘玉华,顾晶晶,刘英,陈海燕,廖嘉宝,伍振峰..抗氧化剂在肉桂挥发油包合物喷雾干燥中的保护作用研究[J].中国中药杂志,2026,51(6):1565-1572,8.基金项目
国家自然科学基金面上项目(82474091) (82474091)
江西省重点研发计划项目(20243BBI91013) (20243BBI91013)
江西中医药大学研究生创新专项(XJ-202503) (XJ-202503)