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芳烃定量用内部标样的制备方法及评价

杨诗妍 图孟格勒 刘保磊 刘勇 郭昱汝 张津铭 赵书逸 文继祖

油气田环境保护2026,Vol.36Issue(2):55-59,65,6.
油气田环境保护2026,Vol.36Issue(2):55-59,65,6.DOI:10.3969/j.issn.1005-3158.2026.02.009

芳烃定量用内部标样的制备方法及评价

Preparation Method and Evaluation of Internal Standard Samples for Aromatic Hydrocarbon Quantification

杨诗妍 1图孟格勒 1刘保磊 2刘勇 1郭昱汝 1张津铭 1赵书逸 1文继祖3

作者信息

  • 1. 中国石油天然气股份有限公司塔里木油田公司实验检测研究院||新疆超深油气重点实验室
  • 2. 长江大学
  • 3. 长江大学||湖南省核地质调查所
  • 折叠

摘要

Abstract

There are currently no published internal standard reference materials for aromatic hydrocarbon quantification specifically aimed at the petroleum industry,which has restricted the development of qualitative and quantitative analysis techniques for aromatic hydrocarbons.This paper introduces the preparation method,quantification method,and quality verification process of internal standards for the quantification of polycyclic aromatic hydrocarbons and their homologues in crude oil.These internal standards for aromatic hydrocarbon quantification can be used for qualitative and quantitative analysis of 19 hydrocarbon components,including naphthalene,phenanthrene,anthracene,pyrene,fluoranthene,benz[a]pyrene,chrysene,benz[a]anthracene,triphenylene,terphenylalkanes,benzohopane,and MTTC(dehydroxylated vitamin E).Using gas chromatography-mass spectrometry,the components of this standard were analyzed for qualitative and quantitative accuracy,homogeneity,and stability,confirming that the standard is uniform and stable.It can be used for quality control of aromatic hydrocarbon analysis,testing methods,oil and gas exploration and development,environmental monitoring,and related scientific research.

关键词

多环芳香烃/标准样品/三芳甾/均一性/稳定性

Key words

polycyclic aromatic hydrocarbons/standard samples/triaromatic steranes/homogeneity/stability

分类

资源环境

引用本文复制引用

杨诗妍,图孟格勒,刘保磊,刘勇,郭昱汝,张津铭,赵书逸,文继祖..芳烃定量用内部标样的制备方法及评价[J].油气田环境保护,2026,36(2):55-59,65,6.

基金项目

科技部项目《中国地球化学油气生物标志物样品库建立和研究》(2001DIA10023) (2001DIA10023)

国家自然基金"沉积盆地有机含硫化合物分子单体碳同位素组成及其生源指示意义"(42572155). (42572155)

油气田环境保护

1005-3158

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