山西中医药大学学报2026,Vol.27Issue(4):378-383,6.DOI:10.19763/j.cnki.2096-7403.2026.04.15
薄层色谱一标多测方法在逍遥丸中的应用
Application of thin-layer chromatography with one standard and multiple measurement method in Xiaoyao Pills
摘要
Abstract
Objective:To establish a thin-layer chromatography with one standard and multiple measurement method for the identification of multiple medicinal materials in Xiaoyao Pills,aiming to control the quality of Chinese patent medi-cine while improving testing efficiency and reducing costs.Methods:Based on the characteristics of components present in different medicinal materials in Xiaoyao Pills,the experiment was carried out by optimizing the preparation method of the test solution,developing the system,and screening different chromogenic agents.One chromatographic system was devel-oped for the simultaneous identification of Danggui and Baizhu,while another system was developed for the simultaneous identification of Baishao and Gancao,thereby establishing a thin-layer chromatography with one standard and multiple measurement method.Results:The thin-layer chromatography spots were clear with good separation and appropriate reten-tion factor(Rf)values.The method demonstrated satisfactory specificity,repeatability and durability.Conclusion:The thin-layer chromatography with one standard and multiple measurement method is scientific,rational,simple and rapid.It can effectively improve testing efficiency and provides a new approach for the identification of Chinese herba preparations con-taining Danggui,Baiazhu,Baishao and Gancao.关键词
逍遥丸/薄层色谱/一标多测Key words
Xiaoyao Pills/thin-layer chromatography/one standard and multiple measurement分类
医药卫生引用本文复制引用
张俊凤,毛婷婷,崔宇宏..薄层色谱一标多测方法在逍遥丸中的应用[J].山西中医药大学学报,2026,27(4):378-383,6.基金项目
国家食品药品监督管理局—国家药品计划抽验项目(食药监稽函[2012]141号第98项) (食药监稽函[2012]141号第98项)