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40%丙硫菌唑·戊唑醇悬浮剂在小麦上的残留行为和膳食风险评估

吴佳欣 吴开婷 宋德灿 江小月 张盈 杨盛江

现代农业研究2026,Vol.32Issue(5):49-54,61,7.
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现代农业研究2026,Vol.32Issue(5):49-54,61,7.

40%丙硫菌唑·戊唑醇悬浮剂在小麦上的残留行为和膳食风险评估

Residual Behavior and Dietary Risk Assessment of Prothioconazole Tebuconazole 40% Suspension Concentrate(SC)in Wheat

吴佳欣 1吴开婷 1宋德灿 1江小月 1张盈 2杨盛江1

作者信息

  • 1. 贵州民族大学 贵州,贵阳 550025
  • 2. 贵州省农业科学院植物保护研究所 贵州,贵阳 550006
  • 折叠

摘要

Abstract

To evaluate the safety of prothioconazole·tebuconazole 40%suspension concentrate(SC)in wheat,the degradation dynamics of the two active ingredients in wheat grains were investigated at four test sites,and the final residues in wheat grains and straws were determined at twelve test sites.A QuEChERS-ultra performance liquid chromatography tandem mass spectrometry(UPLC MS/MS)analytical method was established.The results showed that the average recoveries of prothioconazole and tebuconazole in wheat grain and straw at four spiked levels ranged from 81%to 107%,with relative standard deviations of 0.4%~4.1%.The degradation of both compounds in wheat grains followed first order kinetics,with half lives of 12.8~28.9 d for prothioconazole and 6.5~10.8 d for tebuconazole.The formulation was applied twice at an interval of 7 days at an active ingredient dosage of 210g/hm2.At 35 and 42 days after the last application,the final residues in all regions were below the maximum residue limits(MRL)specified in national standards,and the safety interval was determined to be 35 days.The total dietary risk quotients were 3.91%and 66.07%,respectively,indicating that the dietary risk associated with the use of 40%prothioconazole·tebuconazole SC in wheat is acceptable for the general population.

关键词

小麦/丙硫菌唑/戊唑醇/农药残留/膳食风险

Key words

wheat/prothioconazole/tebuconazole/pesticide residues/dietary risk

分类

农业科技

引用本文复制引用

吴佳欣,吴开婷,宋德灿,江小月,张盈,杨盛江..40%丙硫菌唑·戊唑醇悬浮剂在小麦上的残留行为和膳食风险评估[J].现代农业研究,2026,32(5):49-54,61,7.

基金项目

大学生创新创业训练计划项目(项目编号:202310672063 ()

S202310672061). ()

现代农业研究

2096-1073

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