热力透平2026，Vol.55Issue(2)：102-105,4.DOI:10.13707/j.cnki.31-1922/th.2026.02.004
采用ICP-OES法测定合金钢中的钽
Determination of Tantalum in Alloy Steels by ICP-OES Method
张颖 1尹文轩 1史文斌 1刘思思1
作者信息
- 1. 上海电气电站设备有限公司汽轮机厂,上海 200240
- 折叠
摘要
Abstract
The novel tantalum-containing ferritic heat-resistant steel BW2 is currently being applied in 600℃steam turbines.Alloy steel samples were processed using microwave digestion.Tantalum(Ta)with analytical line of 240.063 nm was selected,and method parameters were optimized to determine Ta in alloy steels using Inductively Coupled Plasma Optical Emission Spectrometry(ICP-OES)method.This method is characterized by its simplicity and convenience.The results indicated that the linear correlation coefficient of the calibration curve exceeded 0.999,and the recoveries ranged from 90.0%to 105.0%.For alloy steels with Ta contents ranging from 0.004 2%to 0.039 0%,the precision could meet the required standards,and the limit of quantification for the method was 0.002 8%.The research findings can provide reference for rapid and accurate determination of Ta in new types of alloy steels,such as BW2.关键词
微波消解法/电感耦合等离子体发射光谱法/合金钢/钽Key words
microwave digestion/Inductively Coupled Plasma Optical Emission Spectrometry(ICP-OES)method/alloy steel/tantalum分类
矿业与冶金引用本文复制引用
张颖,尹文轩,史文斌,刘思思..采用ICP-OES法测定合金钢中的钽[J].热力透平,2026,55(2):102-105,4.
