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微波辅助对桑叶提取物浓缩干燥的协同增效研究

马璐瑶 李研东 李宇航 方天豪 李嘉钰 李剑 常冬梅 牛红日 袁焕青 韩振兴 吴晓菲 韩雪

中国饲料Issue(11):62-72,11.
中国饲料Issue(11):62-72,11.DOI:10.15906/j.cnki.cn11-2975/s.2026020042-05

微波辅助对桑叶提取物浓缩干燥的协同增效研究

Research on the synergistic effect of microwave-assisted concentration and drying of mulberry leaf extracts

马璐瑶 1李研东 2李宇航 1方天豪 1李嘉钰 1李剑 2常冬梅 3牛红日 4袁焕青 3韩振兴 5吴晓菲 1韩雪1

作者信息

  • 1. 河北科技大学食品与生物学院,河北 石家庄 050018
  • 2. 河北省兽药饲料工作总站,河北 石家庄 050035
  • 3. 河北象大合众生物科技有限公司,河北 石家庄 050000
  • 4. 石家庄牧安生物科技有限公司,河北 石家庄 050066
  • 5. 河北众安中兽医药研发有限公司,河北 石家庄 050035
  • 折叠

摘要

Abstract

This study systematically evaluated the effects of different concentration and drying strategies on the quality attributes of mulberry leaf crude extract powder.Conventional rotary evaporation followed by spray drying(SC)was used as the control process.Microwave-assisted processing was introduced to establish four additional combinations,rotary evaporation-hot air drying(XR),rotary evaporation-microwave drying(XW),microwave concentration-hot air drying(WR),and microwave concentration-microwave drying(WW).The samples were comprehensively compared in terms of physicochemical properties,microstructure,retention of major nutritional and bioactive components,and in vitro antioxidant activity.The results demonstrated that the WW treatment exhibited a marked advantage in processing efficiency,with the total concentration and drying time reduced by approximately 90%compared with the XR group.Microwave drying significantly modified the powder microstructure without disrupting the principal chemical backbone.Relative to the SC group,the WW group showed increases of 39%and 49%in soluble protein and polysaccharide contents,respectively.Flavonoid and total phenolic contents reached the highest levels,increasing by 54%and 118%,respectively,while the loss of 1-deoxynojirimycin(1-DNJ)was minimized to approximately 22%.Antioxidant assays indicated that the WW group exhibited the strongest scavenging activities against DPPH∙ and ABTS∙ radicals.Correlation analysis revealed a highly significant positive correlation between ABTS∙ radical scavenging activity and total phenolic content(P<0.01),whereas the correlation between DPPH∙ scavenging activity and phenolic content was comparatively weak though still positive.Principal component analysis further indicated that the concentration method exerted a relatively limited influence on overall sample characteristics,whereas the drying method was the dominant factor driving inter-sample variation and significantly amplified differences among treatments.In conclusion,microwave concentration combined with microwave drying represents an efficient and promising processing strategy for mulberry leaf crude extract powder,providing robust technical support for the industrial production of functional plant-based ingredients.

关键词

桑叶粗提物粉/微波浓缩/微波干燥/营养与活性成分/抗氧化活性

Key words

mulberry leaf crude extract powder/microwave concentration/microwave drying/nutritional and bioactive components/antioxidant activity

分类

农业科技

引用本文复制引用

马璐瑶,李研东,李宇航,方天豪,李嘉钰,李剑,常冬梅,牛红日,袁焕青,韩振兴,吴晓菲,韩雪..微波辅助对桑叶提取物浓缩干燥的协同增效研究[J].中国饲料,2026,(11):62-72,11.

基金项目

中央引导地方科技发展资金项目(246Z2501G) (246Z2501G)

河北省三期现代农业产业技术体系创新团队蛋禽创新团队(HBCT2024260407) (HBCT2024260407)

中国饲料

1004-3314

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