农药科学与管理2026,Vol.47Issue(7):41-45,57,6.
高效液相色谱分析15%呋虫胺·双丙环虫酯微乳剂含量方法研究
Method Development for the Determination of Dinotefuran·Afidopyropen 15% ME
曹俊丽 1梁观凤 2侯影 2张常庆2
作者信息
- 1. 上海悦联化工有限公司,上海 201416
- 2. 上海悦联生物科技有限公司,上海 201512
- 折叠
摘要
Abstract
In this paper,an analytical method was established for the simultaneous determination of dinotefuran and afidopyropen in a 15%micro-emulsions(ME)formulation.Quantitative analysis was performed by high-performance liquid chromatography(HPLC)with a variable-wavelength UV detector at 240 nm,using methanol and water as the mobile phase and a stainless steel column filled with C18(5 μm).The results showed that the linear correlation coefficients of the calibration curves for both analytes were 0.999 95.The standard deviation of 0.064 6%and 0.515 5%,the variation coefficient of 0.011 7%and 0.361 2%,the average recovery of 100.48%and 99.44%were obtained for dinotefuran and afidopyropen,respectively.关键词
呋虫胺/双丙环虫酯/高效液相色谱Key words
dinotefuran/afidopyropen/HPLC分类
农业科技引用本文复制引用
曹俊丽,梁观凤,侯影,张常庆..高效液相色谱分析15%呋虫胺·双丙环虫酯微乳剂含量方法研究[J].农药科学与管理,2026,47(7):41-45,57,6.