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高效液相色谱分析15%呋虫胺·双丙环虫酯微乳剂含量方法研究

曹俊丽 梁观凤 侯影 张常庆

农药科学与管理2026,Vol.47Issue(7):41-45,57,6.
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农药科学与管理2026,Vol.47Issue(7):41-45,57,6.

高效液相色谱分析15%呋虫胺·双丙环虫酯微乳剂含量方法研究

Method Development for the Determination of Dinotefuran·Afidopyropen 15% ME

曹俊丽 1梁观凤 2侯影 2张常庆2

作者信息

  • 1. 上海悦联化工有限公司,上海 201416
  • 2. 上海悦联生物科技有限公司,上海 201512
  • 折叠

摘要

Abstract

In this paper,an analytical method was established for the simultaneous determination of dinotefuran and afidopyropen in a 15%micro-emulsions(ME)formulation.Quantitative analysis was performed by high-performance liquid chromatography(HPLC)with a variable-wavelength UV detector at 240 nm,using methanol and water as the mobile phase and a stainless steel column filled with C18(5 μm).The results showed that the linear correlation coefficients of the calibration curves for both analytes were 0.999 95.The standard deviation of 0.064 6%and 0.515 5%,the variation coefficient of 0.011 7%and 0.361 2%,the average recovery of 100.48%and 99.44%were obtained for dinotefuran and afidopyropen,respectively.

关键词

呋虫胺/双丙环虫酯/高效液相色谱

Key words

dinotefuran/afidopyropen/HPLC

分类

农业科技

引用本文复制引用

曹俊丽,梁观凤,侯影,张常庆..高效液相色谱分析15%呋虫胺·双丙环虫酯微乳剂含量方法研究[J].农药科学与管理,2026,47(7):41-45,57,6.

农药科学与管理

1002-5480

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