农药科学与管理2026,Vol.47Issue(8):39-43,52,6.
200 g/L氟酰羟·苯甲唑悬浮剂的分析方法研究
Analysis of Pydiflumetofen·Difenoconazole 200 g/L SC by HPLC
罗雪婷 1李秋梅 1尹硕 1吴迪 1吕正杰 1潘洪吉1
作者信息
- 1. 北京市植物保护(北京市农药检定所),北京 100029
- 折叠
摘要
Abstract
A high-performance liquid chromatography(HPLC)method was developed for the simultaneous determination of the active ingredients in 200 g/L pydiflumetofen and difenoconazole suspension concentrate(SC).Separation and quantitative analysis of pydiflumetofen and difenoconazole in the samples were achieved using an XBridge BEH C18 column with an acetonitrile-water mixture(70∶30,v/v)as the mobile phase,at a detection wavelength of 230 nm.The results showed good linearity in the range of 0.1~500.0 mg/L,with correlation coefficients(R²)of 1.00 for both analytes.The relative standard deviations(RSD,n=5)were 0.94%and 0.08%,respectively.The average recoveries for pydiflumetofen and difenoconazole,spiked at 3.45 mg and 5.75 mg,were 101.81%and 99.60%,respectively.The detection limits for both compounds were 0.1 mg/L.关键词
氟唑菌酰羟胺/苯醚甲环唑/高效液相色谱法/分析方法Key words
pydiflumetofen/difenoconazole/HPLC/analytical method分类
农业科技引用本文复制引用
罗雪婷,李秋梅,尹硕,吴迪,吕正杰,潘洪吉..200 g/L氟酰羟·苯甲唑悬浮剂的分析方法研究[J].农药科学与管理,2026,47(8):39-43,52,6.