世界有色金属Issue(16)：30-32,3.
硫酸氧铌水解膜过滤制取高纯纳米氧化铌实验研究
Experimental Study on the Preparation of High-purity Nano-sized Niobium Oxide by Hydrolysis Membrane Filtration of Niobium Oxysulfate
摘要
Abstract
The hydrolysis-membrane filtration method of niobium oxysulfate is an important approach for obtaining high-purity ultrafine niobium oxide.Under certain conditions,it can achieve the goal of producing high-purity nano-sized niobium oxide.In traditional techniques,due to the complexity of raw material impurities,especially the excessive content of difficult-to-separate impurities,it becomes particularly challenging to produce high-purity nano-sized niobium oxide relying solely on a single technology.Therefore,a combined approach is needed to address technical issues such as high purity and fine particle size.For this purpose,the hydrolysis-membrane filtration method is jointly applied.Through hydrolysis-membrane filtration,the particle size is maximally controlled and the impurity content is reduced.Based on the principle that niobium and corresponding impurities have different solubilities under certain conditions,special reagents are used for dissolution,and hydrolysis-membrane filtration is employed to maximize the filtration and separation of niobium,removing impurities.By controlling the temperature during calcination,secondary agglomeration is avoided,achieving the goal of producing ultra-high-purity niobium oxide(Nb2O5>99.99％,Sb<5ppm;Si<10ppm)and nano-sized particle size.关键词
水解/膜过滤/高纯/纳米/氧化铌Key words
Hydrolysis/Membrane filtration/High purity/Nano/Niobium oxide分类
化学化工引用本文复制引用
叶思含,梁国安,游宏,梅凌寒,梁昌明..硫酸氧铌水解膜过滤制取高纯纳米氧化铌实验研究[J].世界有色金属,2026,(16):30-32,3.基金项目
九江市9610行动重点科技项目. （）
