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万寿菊花中叶黄素酯的提取及皂化工艺

刘洪海 杜平 梁红兵 张希波 张晓丽

中国食品添加剂Issue(4):129-134,6.
中国食品添加剂Issue(4):129-134,6.

万寿菊花中叶黄素酯的提取及皂化工艺

Study on technologies of extracting and saponifying lutein ester from marigold

刘洪海 1杜平 1梁红兵 1张希波 2张晓丽2

作者信息

  • 1. 新疆中基天然植物纯化高新技术研究院,乌鲁木齐,830002
  • 2. 石河子大学药学院,石河子,832000
  • 折叠

摘要

Abstract

Lutein can be used to improve human immune system and prevent cataract and senile maculutea degeneration.It can be obtained by saponification of lutein ester,which is the major extracts from Marigold.Lutein is widely used in food,food additive,drugs and feed industries.In this paper,extraction of lutein ester from marigold is conducted with n-hexane as extractant.The best condition for saponifying lutein ester was chosen by the orthogonal experiments of L9 (34).It is found that using 20% KOH methanol as the extracting solution,with saponification reaction time of 40 minutes,at a temperature of 50℃,Lutein ester can be thoroughly sponified.Lutein can then be recrystallized in the solvent of acetone and methanol(v : v 1 : 1).The purity of lutein crystal is 97.2%.

关键词

万寿菊/皂化/正交实验/叶黄素酯/叶黄素

Key words

marigold/saponification/orthogonal experiment/lutein ester/lutein

分类

医药卫生

引用本文复制引用

刘洪海,杜平,梁红兵,张希波,张晓丽..万寿菊花中叶黄素酯的提取及皂化工艺[J].中国食品添加剂,2009,(4):129-134,6.

中国食品添加剂

OA北大核心CSTPCD

1006-2513

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