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枸杞低聚糖的分离与结构鉴定

徐鹏 徐德平

食品与发酵工业2009,Vol.35Issue(6):196-198,3.
食品与发酵工业2009,Vol.35Issue(6):196-198,3.

枸杞低聚糖的分离与结构鉴定

Isolation and Structural Determination of Lycium barbarum Oligosaccharide

徐鹏 1徐德平1

作者信息

  • 1. 江南大学食品学院,江苏,无锡,214122
  • 折叠

摘要

Abstract

Lycium barbarum oligosaccharide was extracted with water, Proteins and polysaccharides in the extrac-tion were precipitated by 95% ethanol. Pigment in the extraction was separated by macroporous resin. Oligosaccha-ride was isolated by DE AE-5PW(30) ion-exchange cellulose and HW-55F,HW-40F gel chromatography. Two poly-saccharides Compound were obtained. According to ESI-MS analysis, the average molecular weights of oligosaccha-rides were estimated to be 666.4 and 504.3. Their structures were Fructose(2→4) Glucose(1→2) Glucose α(4→2) Fructose and Galactose β(1→6)Glucose α(1→2) Fructose which were analyzed by NMR.

关键词

枸杞/低聚糖/分离纯化/结构鉴定

Key words

Lycium barbarum,oligosaccharide,isolation,structural determination

分类

轻工纺织

引用本文复制引用

徐鹏,徐德平..枸杞低聚糖的分离与结构鉴定[J].食品与发酵工业,2009,35(6):196-198,3.

食品与发酵工业

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