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利用Design-Expert设计优化木薯渣制备羧甲基纤维素钠工艺研究

林莹 杨有 辛志平

食品工业科技2011,Vol.32Issue(2):289-291,295,4.
食品工业科技2011,Vol.32Issue(2):289-291,295,4.

利用Design-Expert设计优化木薯渣制备羧甲基纤维素钠工艺研究

Design and optimization of preparation of carboxymethyl cellulose with cassava residual by response surface analysis

林莹 1杨有 1辛志平1

作者信息

  • 1. 广西大学轻工与食品工程学院,广西南宁,530004
  • 折叠

摘要

Abstract

The preparation of carboxymethyl cellulose with cassava residual in organic solvent was optimized with Design Expert system. The regression equation expressing the relationship between degree of substitution and the main factors of carboxymethylation was established by stepwise analysis. The R- squared in the model of regression equation was 0.9570. It was indicated that the optimum carboxymethylatione conditions were: 32.7℃ alkalize temperature,the ratio of NaOH/CH2ClCOOH was 2.9,78.5% organic solvent. In these conditions, it was predicted that the highest DS was 0.59,which increased 40% over per-optimization.

关键词

木薯渣/羧甲基纤维素钠/响应面法/取代度

分类

轻工纺织

引用本文复制引用

林莹,杨有,辛志平..利用Design-Expert设计优化木薯渣制备羧甲基纤维素钠工艺研究[J].食品工业科技,2011,32(2):289-291,295,4.

基金项目

广西研究生教育创新计划资助项目. ()

食品工业科技

OA北大核心CSCDCSTPCD

1002-0306

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