食品工业科技2011，Vol.32Issue(2)：338-340,3.
氢化物发生原子荧光法测定灰树花中硒含量
Determination of total selenium in grifola frondosa by hydride generation atomic fluorescence spectrometry
贾婷 1吴向阳 2仰榴青 3肖辉 2邹烨 1魏红2
作者信息
- 1. 江苏大学化学化工学院,江苏镇江,212013
- 2. 江苏大学食品与生物工程学院,江苏镇江,212013
- 3. 江苏大学药学院,江苏镇江,212013
- 折叠
摘要
Abstract
To establish the method of hydride generation-atomic fluorescence spectrometry for the determination of selenium in Grifola frondosa.The best determination conditions including the concentration of carrier hydrochloride, sodium borohydride, medium acid were selected by standard solution.The two kinds of sample pre-treatment methods were compared, the best determination condition was selected.The results revealed that microwave digestion was more complete in sample pre-treatment,which was better than the wet digestion.The linear range was 1～10ng/mL,the detection limit was 0.002ng/mL,the precision was 1.3％～4.1 ％ ( n = 10) ,the recovery rate was 94.96％～97.94％ (n = 5) ,the contents of selenium in Grifola frondosa was 0.2242μg/g.This method could be used to determine selenium in Grifola frondosa.It was accurate, sensitive, simple and rapid.关键词
原子荧光/灰树花/硒分类
轻工纺织引用本文复制引用
贾婷,吴向阳,仰榴青,肖辉,邹烨,魏红..氢化物发生原子荧光法测定灰树花中硒含量[J].食品工业科技,2011,32(2):338-340,3.
