现代食品科技2011，Vol.27Issue(1)：106-108,105,4.
色谱法监测β-D-吡喃葡萄糖苷的合成
Chromatography Technology for Monitoring the Synthesis of β-D-Glucopyranosides
摘要
Abstract
Two glycosidically bond flavor precursors 2,3,4,6-tetraacetyl-geranyl-l-O-β-D-glucopyranoside (GLY-A) and geranyl-β-D-glucopyranoside (GLY-B) were stereo-synthesized by the modified Koenigs-Knorr reaction. Thin layer chromatography (TLC) was used to monitor the reaction. Silica gelcolumn chromatography was used for separating and purifying the samples.By reverse phase HPLC (RP-HPLC), the purity of GLY-A and GLY-B were analyzed as 98.2％ and 96.0％, respectively. The chromatography technology was suitable for the monitoring of the stereo-synthesis of glycosides in monitoring, separation and analysis, obtained an ideal experimental results.关键词
β-D-吡喃葡萄糖苷/香料前体/合成/色谱引用本文复制引用
解万翠,杨锡洪,夏咏梅,陈超平,汤坚..色谱法监测β-D-吡喃葡萄糖苷的合成[J].现代食品科技,2011,27(1):106-108,105,4.基金项目
863科技计划支持项目(2006AA102310) （2006AA102310）
