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离子交换树脂提取糖蜜酒精废液中K~+分离工艺的优化

张平军 于淑娟

食品与发酵工业2009,Vol.35Issue(10):176-180,5.
食品与发酵工业2009,Vol.35Issue(10):176-180,5.

离子交换树脂提取糖蜜酒精废液中K~+分离工艺的优化

Optimization for Extraction of K~+ from Molasses Vinasse by Ion-exchange Resin

张平军 1于淑娟1

作者信息

  • 1. 华南理工大学轻工与食品学院,广东,广州,510640
  • 折叠

摘要

Abstract

Studied of impact ZGC108 resin penetration exchange capacity factors through single factor experiment. The orthogonal test obtained the best optimum conditions were; velocity 1. 2 mL/min, concentration 9. 45 g/L, temperature 298 K and columns filling height 14 cm . At the above condition, the penetrable capability was 52. 98 mg/mL. Variance analysis showed the order of the impact to the penetrating capacity were : velocity > temperature >concentration > height of resin. The velocity and temperature were significant. At the condition of 6BV eluant to resin bed, flow rate 3BV/h , temperature 298 K, 0. 2 mol/L,0. 4 mol/L,0. 6 mol/L of Sulfuric acid used as the eluant,the K~+ eluting were 53. 4% ,78. 6% ,98. 6% respectively; at temperatures 298 K,308 K,318 K of 0. 6 mol/L Sulfuric acid, eluting K~+ were 98.6% ,99.7% ,99.8% separately; it is feasible to recycle the posterior segment of 0. 6mol/L sulfuric acid , at 308 K with the recovery 30% . The research showed the possibility of using molasses vinasse to produce potassium sulfate at low cost.

关键词

糖蜜酒精废液/离子交换/K~+/优化

Key words

molasses vinasse/ ion-exchange resins/ K~+ /optimize

分类

轻工纺织

引用本文复制引用

张平军,于淑娟..离子交换树脂提取糖蜜酒精废液中K~+分离工艺的优化[J].食品与发酵工业,2009,35(10):176-180,5.

基金项目

粤港招标项目"糖蜜发酵废水资源化利用及处理新技术研发"(200849851) (200849851)

食品与发酵工业

OA北大核心CSCDCSTPCD

0253-990X

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