电子元件与材料2011，Vol.30Issue(12)：6-8,3.
柠檬酸溶胶—凝胶法制备Ca2Co2O5粉体及结构表征
Preparation and characterization of Ca2Co2O5 powders by the citrate sol-gel method
摘要
Abstract
Ca2Co2O5 powders were prepared by the sol-gel method using calcium and cobalt nitrates as raw materials, ultrapure water as solvent and citric acid as complexing agent. The optimal process conditions were determined, and the thermal decomposition mechanism of the precursor, the phase and morphology of the Ca2Co2O5 powders were characterized by TG-DSC, XRD, FT-IR, SEM, and EDX. The results show that Ca2Co2O5 powders can be prepared by calcining the xerogel at 700 ℃ for 36 h. Prepared loose powders are sheet-like structure with an average size of 15-20 urn.关键词
热电材料/溶胶—凝胶法/柠檬酸/Ca2Co2O5粉体Key words
thermoelectric materials/ sol-gel method/ citric acid/ Ca2Co2O5 powders分类
矿业与冶金引用本文复制引用
管浩,焦宝祥,于雷..柠檬酸溶胶—凝胶法制备Ca2Co2O5粉体及结构表征[J].电子元件与材料,2011,30(12):6-8,3.基金项目
学校人才引进资助项目(No.XKR2011070) （No.XKR2011070）
