电子与封装2011,Vol.11Issue(8):32-36,5.
溶胶-凝胶法制备高折射GPTMS/TiO_2-ZrO_2材料
Preparation of GPTMS/ TiO_2-ZrO_2 Habrid Materials with High Refractive Index by Sol-gel Process
摘要
Abstract
Nanocomposites hybrid materials of GPTMS/TiO2-ZrO2 with high refractive index and transparency were synthesized through Sol-Gel method,tetrabutoxytitanate and zirconium n-tetrabutanoxide including γ-Glycidoxypropyl trimethoxysilane(GPTMS) were employed as sources of the titania-zirconia sol and the silica sol,respectively.Subsequently,hybrid films were abtain with thermal curing crosslinking after spin coating or dip-coating on glass substrates.The hybrid ?lms have been characterized via FTIR,AFM,UV-vis,ellipsometer etc.The results indicated that the hybrid ?lms displayed homogeneous morphology and transmittances are higher than 91% in the visible range.RI of the films increased from 1.491 to 1.618 at 632.8nm titania-zirconia mass fraction from 10% to 50 %.关键词
溶胶-凝胶法/TiO2-ZrO2/高折射率/杂化材料Key words
sol-gel mathod/TiO2-ZrO2/high refractive index/hybrid materials分类
信息技术与安全科学引用本文复制引用
黄敏,黄佐华,林晓丹,曾幸荣,李巧龙,刘志猛,刘煜平..溶胶-凝胶法制备高折射GPTMS/TiO_2-ZrO_2材料[J].电子与封装,2011,11(8):32-36,5.基金项目
东莞市高等院校科研机构科技计划重点项目,项目编号:201010814002 ()