肉类研究Issue(10)：29-31,3.
高效液相色谱法测定猪肉中氟喹诺酮类药物
Determination of Fluoroquinolone Residues in Pork by HPLC
摘要
Abstract
An HPLC with FLD （fluorescence detector） method was established for the determination of two kinds of fluoroquinolones in pork. Pork samples were extracted with 1% acetic acid/acetonitrile, followed by water removal by anhydrous sodium sulfate and clean-up by acetonitrile saturated n-hexane. The mobile phase was composed of acetonitrile and 0.01 mol/L sodium phosphate （pH 3, adjusted with phosphorous acid） at a ratio of 10：90 （V/V）. The analytes were separated on a ZORBAX-SB-CIs column and detected by a fluorescence detector. The established method proved accurate, rapidy and sensitive.关键词
高效液相色谱法/氟喹诺酮类药物/残留分析/猪肉Key words
high performance liquid chromatography （HPLC）/fluoroquinolone/residue analysis/pork分类
化学化工引用本文复制引用
朱莉萍,朱涛,武娜,倪永付,王勇,闫秋成..高效液相色谱法测定猪肉中氟喹诺酮类药物[J].肉类研究,2011,(10):29-31,3.基金项目
山东出入境检验检疫局科技项目 （）
