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超临界体系酶法催化甘油解制备甘油二酯的研究

任运宏 孙博 刘晶 江连洲 于殿宇

食品工业科技Issue(10):337-340,4.
食品工业科技Issue(10):337-340,4.

超临界体系酶法催化甘油解制备甘油二酯的研究

Study on enzymatic synthesis of diacylglycerol by glycerolysis in supercritical system

任运宏 1孙博 1刘晶 1江连洲 1于殿宇1

作者信息

  • 1. 东北农业大学食品学院,黑龙江哈尔滨150030
  • 折叠

摘要

Abstract

The preparation of DG by enzymatic glycerolysis in the CO2 supercritical system was studied. The effect of substrate soybean oil/glycerin molar ratio,temperature,amount of enzyme,water content of glycerol, time and stirring speed on the preparation of DG were studied. Through the single factor and orthogonal tests, the optimum conditions were determined as follows: ubstrate molar ratio 2:1, temperature 65℃, amount of enzyme 2.5%,water content of glycerol 1%, time 7h, stirring speed 120r/min. The product content of DG were 70.2% ,of which 1,3-DG were 56.2%. Compared with the conventional glycerolysis,the content of DG were much more than 7%, of which 1,3-DG were much more than 5%,and time reduced about two hours.

关键词

大豆油/甘油解/脂肪酶/Lipozyme/RM^IM/CO2超临界/甘油二酯

Key words

soybean oil/glycerolysis/lipase Lipozyme RM^IM/CO2 supercritical/diacylglycerol

分类

轻工纺织

引用本文复制引用

任运宏,孙博,刘晶,江连洲,于殿宇..超临界体系酶法催化甘油解制备甘油二酯的研究[J].食品工业科技,2011,(10):337-340,4.

基金项目

基金项目:国家863高技术研究发展计划(2010AA101503). ()

食品工业科技

OA北大核心CSCDCSTPCD

1002-0306

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