食品工业科技Issue(11):120-122,3.
火麻仁油中脂肪酸的不同酯化方法与GC-MS分析
Analysis of fatty acids in hemp seed oil using three different esterification methods by GC-MS
李文峰 1汪晓伟 1刘飞 1戴煌 1方国珊 1明建1
作者信息
摘要
Abstract
The hemp seed oil was extracted by Soxhletex traction.The fatty acids in the hemp seed oil were esterified by three methods and analyzed by gas chromatography-mass spectrometry(GC-MS).The components and their relative contents of the fatty acids were compared with each other.The results showed that 14 fatty acids were identified by esterification method 1,11 fatty acids were identified by esterification method 2 and 10 fatty acids were identified by esterification method 3.The contents of the identified fatty acids accounted for 83.36%,99.63% and 96.98% of the hemp seed oil,respectively.Comparison of the major fatty acids was made:the major fatty acids were hexadecanoic acid(10.97%),octadecanoic acid(7.56%),9,12-octadecadienoic acid(13.42%)and 9-octadecenoicacid(34.80%)by esterification method 1.The major fatty acids were hexadecanoic acid(8.33%),octadecanoic acid(5.53%),9,12-octadecadienoic acid(54.64%)and 9,12,15-octadecatrienoic acid(25.42%)by esterification method 2.The major fatty acids were hexadecanoic acid(8.20%),octadecanoic acid(5.23%),9,12-octadecadienoic acid(52.19%)and 9,12,15-octadecatrienoic acid(25.77%)by esterification method 3.关键词
火麻仁/脂肪酸/酯化方法/气相色谱-质谱联用Key words
hemp seed oil/fatty acid/esterification methods/GC-MS分类
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李文峰,汪晓伟,刘飞,戴煌,方国珊,明建..火麻仁油中脂肪酸的不同酯化方法与GC-MS分析[J].食品工业科技,2011,(11):120-122,3.