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电化学法测定玉米油酸价的不确定度评定

张春娥 薛文通

食品工业科技Issue(1):329-331,3.
食品工业科技Issue(1):329-331,3.

电化学法测定玉米油酸价的不确定度评定

Uncertainty evaluation of determination of acid value in corn oil using electrochemical detection

张春娥 1薛文通2

作者信息

  • 1. 中国农业大学食品科学与营养工程学院,北京100083 宁夏粮油产品质量检测中心,宁夏银川750002
  • 2. 中国农业大学食品科学与营养工程学院,北京100083
  • 折叠

摘要

Abstract

According to JJF 1059-1999 'Evaluation and Expression of Measurement Uncertainty',analyzed the source of uncertainty for electrochemical detection,calculated relative expanded standard uncertainty of corn oil acid value.The uncertainty was caused by many factors,such as electronic weighing scales μ1,glass container μ2,SNR μ3,repeatability of measurement result for standard solution μ4,sample measurement μ5,standard curve μ6 and recovery rate μ7.The results showed that the acid value obtained by electrochemical detection was 0.52mg KOH/g oil and relative value was 0.068mg/g,relative expanded standard uncertainty was 26.2%.

关键词

电化学法/酸价/玉米油/不确定度评定

Key words

electrochemical detection/acid value/corn oil/uncertainty evaluation

分类

轻工纺织

引用本文复制引用

张春娥,薛文通..电化学法测定玉米油酸价的不确定度评定[J].食品工业科技,2012,(1):329-331,3.

基金项目

公益性行业科研专项 ()

国家自然基金 ()

食品工业科技

OA北大核心CSCDCSTPCD

1002-0306

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