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一步提取测定食品中的脂肪酸

黄菲菲 赵嘉胤 王建军 陈景春

食品工业科技Issue(2):77-79,3.
食品工业科技Issue(2):77-79,3.

一步提取测定食品中的脂肪酸

Determination of fatty acids in foods by one-step extraction

黄菲菲 1赵嘉胤 1王建军 1陈景春1

作者信息

  • 1. 农业部食品质量监督检验测试中心(上海),上海200436
  • 折叠

摘要

Abstract

A method of one-step extraction determination of fatty acids in foods by gas chromatography(GC) was developed.Samples were esterified by hydrochloric acid-methanol, which was the reaction product of acetyl chloride and methanol.Extracting with toluene, contents of fatty acids were determined by GC with FID detector.The method had a good linear relativity( r = 0.999)between 0.005-1 mg/mt Recovery rate in different samples range from 82.1% to 100%, RSD 〈 10% ,with the LOD of lmg/100g.With the advantages of easy-handling,fast and high sensitivity,one-step extraction method could meet the requirement of the determination of fatty acids in foods.

关键词

脂肪酸/气相色谱/一步提取/食品

Key words

fatty acids/G C/one-step extraction/foods

分类

轻工纺织

引用本文复制引用

黄菲菲,赵嘉胤,王建军,陈景春..一步提取测定食品中的脂肪酸[J].食品工业科技,2012,(2):77-79,3.

食品工业科技

OA北大核心CSCDCSTPCD

1002-0306

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