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微波消解-电感耦合等离子体发射光谱法测定茶叶中的镉

杨秀芳 许凌 徐建峰 涂云飞 孔俊豪

食品科学2011,Vol.32Issue(18):218-220,3.
食品科学2011,Vol.32Issue(18):218-220,3.

微波消解-电感耦合等离子体发射光谱法测定茶叶中的镉

Determination of Cadmium in Tea Using Microwave Digestion and Inductively Coupled Plasma Atomic Emission Spectroscopy

杨秀芳 1许凌 1徐建峰 2涂云飞 1孔俊豪2

作者信息

  • 1. 中华全国供销合作总社杭州茶叶研究院,浙江杭州310016
  • 2. 国家茶叶质量监督检验中心,浙江杭州310016
  • 折叠

摘要

Abstract

The contents of cadmium in tea samples including green tea,oolong tea,jasmine tea,and Pu,er tea were determined using microwave digestion followed by inductively coupled plasma atomic emission spectroscopy(ICP-AES).The linear range was from 0 to 100μg/L(R2 = 0.9998).The limit of detection(LOD) for cadmium was 1.88μg/L.The spike recovery was ranged from 95.7% to 102.3% with a relative standard derivation(RSD) of 1.1%.In conclusion,the method is a rapid,convenient,and highly sensitive method to determine cadmium content in tea samples.The contents of cadmium in randomly sampled forty tea samples were between 0.017 mg/kg and 0.138 mg/kg with an average of(0.082±0.028) mg/kg.The average content of cadmium in green tea showed a significant difference when compared with other tea samples(P0.05).

关键词

茶叶//微波消解/电感耦合等离子体发射光谱(ICP-OES)

Key words

tea/cadmium/microwave digestion/inductively coupled plasma atomic emission spectroscopy(ICP-OES)

分类

资源环境

引用本文复制引用

杨秀芳,许凌,徐建峰,涂云飞,孔俊豪..微波消解-电感耦合等离子体发射光谱法测定茶叶中的镉[J].食品科学,2011,32(18):218-220,3.

基金项目

浙江省分析测试基金项目 ()

食品科学

OA北大核心CSCDCSTPCD

1002-6630

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