食品科学2011，Vol.32Issue(18)：268-273,6.
QuEChERS-GC/MS快速检测柑橘中50种农药残留
Rapid Determination of 50 Pesticide Residues in Citrus by QuEChERS-Gas Chromatography-Mass Spectrometry
摘要
Abstract
An analytical method for the rapid determination of 50 pesticides residues in citrus by gas chromatography-mass spectrometry（GC-MS） with QuEChERS was established in a selected ion-monitoring（SIM） mode.The pesticide residues in samples were extracted into acetonitrile and salted out by anhydrous MgSO4 and NaCl.Then,the pesticide residues in the supernatant after clean-up on N-propyl ethylenediamine（PSA） cartridge were subjected to GC-MS analysis.Under the optimal conditions,the limits of detection（RSN = 3） of the established method were in the range of 0.0038-0.066 mg/kg,and the average recovery rates（n=6） for 50 pesticide residues in a blank sample were 72.0%-118.2% with a relative standard deviations（RSDs） of 1.7%-19.7%.关键词
柑橘/QuEChERS/气相色谱-质谱/多残留分析Key words
citrus/QuEchERS/gas chromatography-mass spectrometry（GC-MS）/multiple pesticide residue analysis分类
化学化工引用本文复制引用
黄霞,宋莹,张耀海,李云成,焦必宁..QuEChERS-GC/MS快速检测柑橘中50种农药残留[J].食品科学,2011,32(18):268-273,6.基金项目
“十一五”国家科技支撑计划项目（2007BAD47B07 （）
2009BADB7B04） （）
国家现代农业（柑桔）产业技术体系建设专项 （）
重庆市自然科学基金项目 （）
柑桔学重庆市市级重点实验室开放基金项目 （）
