食品科学2012，Vol.33Issue(2)：173-176,4.
离子色谱法直接测定食品添加剂中的甜蜜素
Direct Determination of Sodium Cyclamate in Food Additives by Ion Chromatography
朱怀远 1庄亚东 1熊晓敏 1万敏 1沈晓晨 1张映1
作者信息
- 1. 江苏中烟工业有限责任公司技术研发中心,江苏南京210019
- 折叠
摘要
Abstract
A new method was developed for direct determination of sodium cyclamate in food additives by ion chromatograph coupled with electrical conductivity detector based on high water solubility and ionization characteristics of sodium cyclamate.Sodium cyclamate in samples were extracted into deionized water by shaking,separated on an anion exchange column using 30 mmol/L KOH aqueous solution as elution solvent and detected by an electrolytic conductivity detector.The method showed good linearity over the concentration range of 5-200μg/mL with a correlation coefficient of 0.9999 and a detection limit of 0.087μg/mL.The intraday and inter-day relative standard deviations（RSDs） were less than 3% and 2% respectively.The method was simple and stable without complex sample pretreatment,and allowed easy,rapid and accurate determination of sodium cyclamate in food additives.关键词
离子色谱法/食品添加剂/甜蜜素Key words
ion chromatography/food additives/sodium cyclamate分类
化学化工引用本文复制引用
朱怀远,庄亚东,熊晓敏,万敏,沈晓晨,张映..离子色谱法直接测定食品添加剂中的甜蜜素[J].食品科学,2012,33(2):173-176,4.
