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不同年生西洋参中20种有机氯农药的气相色谱分析

秦公伟 曹小勇 耿敬章 张静 陈玉芳 陈富东

食品科学2012,Vol.33Issue(2):199-203,5.
食品科学2012,Vol.33Issue(2):199-203,5.

不同年生西洋参中20种有机氯农药的气相色谱分析

Determination of Organochlorine Pesticides in Panax quinquefolium L. with Different Ages by Gas Chromatography

秦公伟 1曹小勇 1耿敬章 1张静 2陈玉芳 1陈富东1

作者信息

  • 1. 陕西理工学院生物科学与工程学院,陕西省资源生物重点实验室,陕西汉中723001
  • 2. 陕西理工学院历史文化与旅游学院,陕西汉中723001
  • 折叠

摘要

Abstract

a high performance gas chromatography method has been developed for determining 20 kinds of organochlorine pesticides including α-BHC and 4,4'-DDT in American ginseng(Panax quinquefolium L.) grown in different areas of GAP plantation base from Liuba county,shaanxi province.The accumulation of organochlorine pesticides in American ginseng with different ages was also explored.Organochlorine pesticides in samples were extracted by hexane-ethyl acetate(1:1) solution,and then purified by a column packed with Florisil using hexane-ethyl acetate(1:1) as elution solvent.Chromatographic analysis was performed on a DB-17 capillary column supplemented with electron capture detector(ECD).A total of 19 organochlorine pesticides except for endrin were detected.The contents of organochlorine pesticides in samples from different areas revealed an obvious difference.Moreover,the residues of organochlorine pesticides in four-year-old American ginseng were higher than those in three-year-old or five-year-old American ginseng.Therefore,this developed method is effective,fast and accurate,which can be used for determining 20 kinds of organochlorine pesticides in American ginseng.

关键词

西洋参/有机氯农药/气相色谱法

Key words

Panax quinquefolium L./organochlorine pesticides/gas chromatography

分类

医药卫生

引用本文复制引用

秦公伟,曹小勇,耿敬章,张静,陈玉芳,陈富东..不同年生西洋参中20种有机氯农药的气相色谱分析[J].食品科学,2012,33(2):199-203,5.

基金项目

陕西省科技厅重点项目 ()

陕西省教育厅资源生物省级重点实验室项目 ()

食品科学

OA北大核心CSCDCSTPCD

1002-6630

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