食品科学2012，Vol.33Issue(2)：208-210,3.
离子色谱直接电导法检测糖蜜中的甜菜碱
Determination of Betaine in Molasses by Ion Chromatography with Direct Conductivity Detection
张晨光 1潘见 2黄文平 3杨毅2
作者信息
- 1. 合肥工业大学农产品生物化工教育部工程研究中心,安徽合肥230009／安徽皖仪科技股份有限公司,安徽合肥230088
- 2. 合肥工业大学农产品生物化工教育部工程研究中心,安徽合肥230009
- 3. 安徽皖仪科技股份有限公司,安徽合肥230088
- 折叠
摘要
Abstract
An ion chromatography-direct conductivity detection method was developed for determining betaine in molasses.The chromatographic separation of betaine was achieved on a WY cation column（150 mm × 4.6 mm i.d.） using 2.0 mmol/L MSA as mobile phase at a flow rate of 1.0 mL/min.The column was set at 30 ℃.Betaine was detected using a direct conductivity detector.A good linear range of the calibration curve was achieved over the concentration of 0.5-50 mg/L（r = 0.9995） with recovery rate of 93.5%-99.7% and detection limit of 0.15 mg/L.The method was suitable for the determination of betaine and quality control for betaine extraction from molasses.关键词
离子色谱/直接电导/糖蜜/甜菜碱Key words
ion chromatography/direct conductivity detection/betaine/molasses分类
轻工纺织引用本文复制引用
张晨光,潘见,黄文平,杨毅..离子色谱直接电导法检测糖蜜中的甜菜碱[J].食品科学,2012,33(2):208-210,3.
