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高纯度共轭亚油酸的制备

徐达 陈华勇 罗日明 王卫飞 杨博

食品与发酵工业2011,Vol.37Issue(6):110-113,4.
食品与发酵工业2011,Vol.37Issue(6):110-113,4.

高纯度共轭亚油酸的制备

Research on the Preparation Method of High Purity Conjugated Linoleic Acid

徐达 1陈华勇 1罗日明 1王卫飞 2杨博1

作者信息

  • 1. 华南理工大学生物科学与工程学院,广东广州510006
  • 2. 华南理工大学轻工与食品学院,广东广州510640
  • 折叠

摘要

Abstract

High purity conjugated linoleic acid(CLA) was prepared by means of urea adduct purification and conjugation by safflower oil.This paper is focused on two different synthesis methods:(1) alkaline catalysis-urea adduction fractionation,(2) saponification-urea adduction fractionation-alkaline catalysis.The processing parameters and the ratio of CLA isomers for each method were investigated.The result showed that the second method which was enriching linoleic acid(LA) first and then performing alkaline catalyzed conjugation was better.Under the optimal conditions,CLA of 97.22% purity was achieved;the total recovery of the product was 32.08%,the content of c9,t11-CLA and t10,c12-CLA were 45.14% and 49.12% respectively.

关键词

共轭亚油酸/高纯度/尿素包合/碱法异构

Key words

CLA/high purity/urea adduction fractionation/alkaline catalysis

分类

轻工纺织

引用本文复制引用

徐达,陈华勇,罗日明,王卫飞,杨博..高纯度共轭亚油酸的制备[J].食品与发酵工业,2011,37(6):110-113,4.

基金项目

广东省科技攻关项目 ()

广州市重大科技攻关项目 ()

食品与发酵工业

OA北大核心CSCDCSTPCD

0253-990X

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