食品与发酵工业2011，Vol.37Issue(10)：174-177,4.
茶叶、茶鲜叶及茶汤中啶虫脒残留的检测
A Method for Determination of Acetamiprid Residue in Tea, Fresh Tea and Tea Infusion with HPLC-UV
摘要
Abstract
An effective method was developed for analysis of acetamiprid residue in tea, fresh tea and tea infusion by high performance liquid chromatography（HPLC）with UV detector. Tea samples were extracted by acetonitrile and Nacl Alkaline saturated solution, then purified with the Envi - Carb/NH2 cartridge, finally eluted with 10ml acetonitrile. Imidcloprid recoveries in tea, fresh tea were in the range of 68.5% -103.6% with 0.1 -1.0mg/kg acetamiprid and relative standard deviations （RSD）. when acetamiprid content was 0. 033 -0. 333mg/L in infusion, The recovery was 73% - 103.8% with RSD less than 7.6%. Practical determination limit in tea, fresh tea and infusion respectively was 0.07mg/kg, 0.09mg/kg and 0. 002mg/L. the method is quick and effective. It can be used for routine monitoring of the acetamiprid residues and safety assessment research in the tea.关键词
啶虫脒/农药残留/高效液相色谱/固相萃取/茶叶Key words
acetamiprid/pesticide residues/HPLC/solid-phase extraction/tea分类
轻工纺织引用本文复制引用
苏婷,侯如燕,赵秀霞,钱晓三,杨婷婷..茶叶、茶鲜叶及茶汤中啶虫脒残留的检测[J].食品与发酵工业,2011,37(10):174-177,4.基金项目
农业部现代农业产业技术体系（农科教发[2008]10号）及张一元科技创新基金项目资助 （）
