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椪柑籽油超临界提取工艺的优化

何阳 夏延斌

食品与机械2012,Vol.28Issue(1):178-182,5.
食品与机械2012,Vol.28Issue(1):178-182,5.DOI:10.3969/j.issn.1003-5788.2012.01.047

椪柑籽油超临界提取工艺的优化

Research and optimization on ponkan seed extracting by supercritical CO2 fluid extraction technique

何阳 1夏延斌2

作者信息

  • 1. 湖南农业大学食品科技学院,湖南长沙410128
  • 2. 湖南省农产品加工研究所,湖南长沙410125
  • 折叠

摘要

Abstract

The influences of time, temperature, pressure and the flux of CO2 on the yield of seed oil from its powder with the supercritical CO2 fluid extraction technique were studied according to the Box-Be-hnken central composite experimental design based on the single factor test. Analyzed the mathematical model which established by response surface methodology ( RSM), and the same time, relationships between studied factors and response of Ponkan seed oil extraction yield were described. Based on the canonical analysis, the optimum conditions were obtained as follows: the extraction pressure is 34. 4 Mpa, the flow rate of CO2 25. 8 L/h, the extraction time is 147. 6 min and the temperature 39. 3 °C. Under the optimized extraction conditions, the predictive maximum yield, of seed oil was 45.95% and the average validation value was (45. 12 + 1. 36) % (n = 3) , so the model could be used to predict the extraction results well.

关键词

椪柑籽/超临界CO2萃取/工艺优化

Key words

ponkan seed/ supercritical CO2 fluid extraction/ processes optimization

引用本文复制引用

何阳,夏延斌..椪柑籽油超临界提取工艺的优化[J].食品与机械,2012,28(1):178-182,5.

基金项目

国家863计划(编号:2007AA10Z307) (编号:2007AA10Z307)

湖南省产学研结合专项(编号:2009XK6001) (编号:2009XK6001)

食品与机械

OA北大核心CSCDCSTPCD

1003-5788

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