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离子液体[Bmim]Cl预处理对两种高结晶多糖酸水解的影响

李娜 王兆梅 肖凯军

食品工业科技2012,Vol.33Issue(7):302-304,308,4.
食品工业科技2012,Vol.33Issue(7):302-304,308,4.

离子液体[Bmim]Cl预处理对两种高结晶多糖酸水解的影响

Effect of ionic liquid pretreatment step on acid hydrolysis of two high crystallization polysaccharide

李娜 1王兆梅 1肖凯军1

作者信息

  • 1. 华南理工大学轻工与食品学院,广东广州510640
  • 折叠

摘要

Abstract

The effect of an ionic liquid 1-butyl-3-methylimidazoliumchloride([Bmim]Cl)pretreatment on the efficiency of the acid hydrolysis and crystallinity of brewer yeast-β-glucans and curdlan was investigated by using polarized optical microscope,X-ray diffraction(XRD)and 3,5-dinitrosalicylic acid(DNS)method.It was demonstrated from the XRD spectrometry that the crystallinity of brewer yeast-β-glucans and curdlan declined dramatically with ionic liquid pretreated.Brewer yeast-β-glucans and curdlan pretreated with[Bmim]Cl enhanced the efficiency and increased the reducing sugar content during the acid hydrolysis.The reducing sugar content of brewer yeast-β-glucans(acid hydrolysis for 2h)and curdlan(acid hydrolysis for 3h)with the ionic liquid pretreated were 84.36g/100g and 96.07g/100g respectively,much higher than that of the untreated samples which were 53.44g/100g and 46.80g/100g in 4mol/L TFA at 100℃.

关键词

酵母β-葡聚糖/凝结多糖/离子液体/酸水解

Key words

brewer yeast-β-glucans/curdlan/ionic liquid/acid hydrolysis

分类

轻工纺织

引用本文复制引用

李娜,王兆梅,肖凯军..离子液体[Bmim]Cl预处理对两种高结晶多糖酸水解的影响[J].食品工业科技,2012,33(7):302-304,308,4.

基金项目

国家自然科学基金资助项目 ()

华南理工大学中央高校基本科研业务费专项资金项目 ()

食品工业科技

OA北大核心CSCDCSTPCD

1002-0306

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