食品科学2012，Vol.33Issue(4)：148-152,5.
薏苡仁中多种农药残留的测定
Determination of Multiple Pesticide Residues in Coix Seed
李俊 1王震 1庞宏宇 1郭晓关 1任玉娟 1吴旭刚1
作者信息
- 1. 贵州省农产品质量安全监督检验测试中心,农业部农产品质量安全监督检验测试中心（贵阳）,贵州贵阳550004）
- 折叠
摘要
Abstract
A method to simultaneously determine 43 pesticide residues in coix seed is described in this paper. Samples were extracted by accelerated solvent extraction （ASE）, cleaned up by either solid phase extraction （SPE） or gel permeation chromatography （GPC）, and analyzed by gas chromatography-mass spectrometry （GC-MS）. The spike recoveries obtained by SPE and GPC were 72.45% - 111.74% and 74.70% - 106.49%, and the RSDs 1.47% - 5.06% and 1.58% - 5.08%, respectively. Correlation coefficients between 1.47% and 5.06% were found for the established calibration curves. The limits of detection （LOD） of the method varied from 0.002 to 0.02 mg/kg, and the limits of quantification （LOQ） from 0.005 to 0.05 mg/kg. The method was efficient, accurate, sensitive and applicable for the simultaneous determination of multiple pesticide residues in coix seed.关键词
薏苡仁/农药残留/快速溶剂萃取仪/固相萃取/凝胶渗透色谱/气相质谱联用仪Key words
coix seed: pesticide residue: accelerated solvent extraction (ASE)/solid phase extraction (SPE): gelpermeation chromatography (GPC)/gas chromatography-mass spectrometry (GC-MS)分类
农业科技引用本文复制引用
李俊,王震,庞宏宇,郭晓关,任玉娟,吴旭刚..薏苡仁中多种农药残留的测定[J].食品科学,2012,33(4):148-152,5.
