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搅拌棒磁子萃取-热脱附-气相色谱质谱联用分析葫芦巴浸膏的挥发性成分

苏勇 冒德寿 曲荣芬 李智宇 毛多斌

食品工业科技2012,Vol.33Issue(13):78-80,83,4.
食品工业科技2012,Vol.33Issue(13):78-80,83,4.

搅拌棒磁子萃取-热脱附-气相色谱质谱联用分析葫芦巴浸膏的挥发性成分

Analysis of volatile components in fenugreek extract( Trigonella foenum-graecum L) by stir bar sorptive extraction-thermal desorption and gas chromatography-mass spectrometry

苏勇 1冒德寿 2曲荣芬 2李智宇 2毛多斌3

作者信息

  • 1. 郑州轻工业学院食品与生物工程学院,河南郑州450002/红塔烟草集团有限责任公司技术中心,云南玉溪653100
  • 2. 红塔烟草集团有限责任公司技术中心,云南玉溪653100
  • 3. 郑州轻工业学院食品与生物工程学院,河南郑州450002
  • 折叠

摘要

Abstract

Volatile components from fenugreek extract were analyzed by using stir bar soptive extraction-thermal desoption and gas chromatography-mass spectrometry,and sixty-seven compounds were identified. 1,2- propylene glycol (38.83%), 2-phenylethyl2-phenylacetate (7.32%) ,2,4-dimethy1-1,3-dioxolane-2-methanol (5.33%), rinalool (3.67%) ,2-acetoxy- 1 -propanol (3.54%), isovaleric acid (2.75%) and 2-acetylfuran (2.06%) were the main components. In addition,the flavor mechanism was discussed. The research provided technological basis for quality control and exploit of fenugreek extract.

关键词

葫芦巴浸膏/搅拌棒磁子萃取/热脱附/气质联用/挥发性成分

Key words

fenuqreek extract/stir bar sorptive extraction/TDU/GC-MS/volatile components

分类

轻工纺织

引用本文复制引用

苏勇,冒德寿,曲荣芬,李智宇,毛多斌..搅拌棒磁子萃取-热脱附-气相色谱质谱联用分析葫芦巴浸膏的挥发性成分[J].食品工业科技,2012,33(13):78-80,83,4.

基金项目

国家烟草专卖局卷烟增香保润重大专项研究项目(110200902020). ()

食品工业科技

OA北大核心CSCDCSTPCD

1002-0306

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