食品与发酵工业2012，Vol.38Issue(5)：185-190,6.
不同前处理-石墨炉原子吸收光谱法检测红葡萄酒中铅
Determination of Lead in Red Wine by Different Pre-treatment Graphite Furnace Atomic Absorption Spectrometry
摘要
Abstract
Plum bum （Pb） determination in red wine by graphite furnace atomic absorption spectrometry （GF-AAS） was established through the research of pre-treatment method. The optimum conditions for determination of Pb in red wine were studied by five different pre-treatments. Result showed that the best matrix modifier agent was aseor-bic acid, its inhalation volume was 51μL. These pre-treatments were： direct dilution, evaporation concentration, H202-HNO3 digestion, HCIO4-HNO3 digestion and microwave digestion. The standard deviation was about 5% ; the microwave dispels RSD was 3.2%. This method is rapid and accurate and can be used in the detection of Pb.关键词
石墨炉原子吸收/红葡萄酒/微波消解/铅Key words
graphite furnace atomic absorption spectrometry/red wine/microwave digestion/lead分类
轻工纺织引用本文复制引用
郭金英,李丽,任国艳,殷勇..不同前处理-石墨炉原子吸收光谱法检测红葡萄酒中铅[J].食品与发酵工业,2012,38(5):185-190,6.基金项目
河南科技大学博士科研启动基金（2006050）,河南省教育厅自然科学研究计划项目（2011A330001）,河南科技大学实验技术开发基金项目（SY0809048）,河南科技大学青年科研基金（2007QN013）项目资助 （）
