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顶空固相微萃取-气质联用法测定哈尔滨红肠的挥发性风味物质

潘丽军 何宇洁 蔡克周 姜绍通

食品科学2012,Vol.33Issue(10):232-236,5.
食品科学2012,Vol.33Issue(10):232-236,5.

顶空固相微萃取-气质联用法测定哈尔滨红肠的挥发性风味物质

Volatile Analysis of Harbin Sausage by Head Space Solid Phase Microextraction and Gas Chromatography-Mass Spectrometry

潘丽军 1何宇洁 1蔡克周 1姜绍通1

作者信息

  • 1. 合肥工业大学生物与食品工程学院,安徽省农产品精深加工重点实验室,安徽合肥230009
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摘要

Abstract

The volatile flavor compounds in Harbin Sausage was extracted by head space solid phase microextraction (HS- SPME) technique and determined by capillary gas chromatography-mass spectrometry (GC-MS). The types of SPME fibers, extraction time, and extraction temperature were optimized in this study. The optimum extraction conditions were obtained as follows: 50/30 μm DVB/CAR/PDMS fiber, adsorption time was 50min at 50℃. Aldehydes, ketones, phenols, alcohols, terpenes, alkanes, sulfur compounds and heterocyclic compounds were the major flavor compounds of Harbin Sausage with relative content of 17.59%, 7.01%, 7.27%, 12.29%, 9.39%, 6.14%, 27.38%, 7.01%, respectively.

关键词

顶空固相微萃取/气质联用/挥发性风味物质/哈尔滨红肠

Key words

head space solid phase microextraction/gas chromatography-mass spectrometry/volatile flavor compounds:harbin Sausage

分类

轻工纺织

引用本文复制引用

潘丽军,何宇洁,蔡克周,姜绍通..顶空固相微萃取-气质联用法测定哈尔滨红肠的挥发性风味物质[J].食品科学,2012,33(10):232-236,5.

基金项目

安徽省战略性新兴产业项目 ()

食品科学

OA北大核心CSCDCSTPCD

1002-6630

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