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顶空固相微萃取结合GC-O与GC-MS技术鉴定可可粉中特征风味化合物

肖天鹏 郑晓峰 吕吉鸿 郭泽峰 高峰 刘春凤 李崎

食品工业科技2012,Vol.33Issue(18):67-69,72,4.
食品工业科技2012,Vol.33Issue(18):67-69,72,4.

顶空固相微萃取结合GC-O与GC-MS技术鉴定可可粉中特征风味化合物

Identification of characteristic flavor compounds in cocoa powder by gas chromatography-olfactometry-mass spectrometry with headspace solid phase micro-extraction

肖天鹏 1郑晓峰 2吕吉鸿 2郭泽峰 2高峰 2刘春凤 1李崎1

作者信息

  • 1. 江南大学工业生物技术教育部重点实验室,江苏无锡214122 江南大学酿酒科学与工程研究室,江苏无锡214122
  • 2. 杭州千岛湖啤酒有限公司,浙江淳安311700
  • 折叠

摘要

Abstract

A method for headspace solid-phase microextraction(HS-SPME),followed by gas chromatography-olfactometry-mass spectrometry analysis was established for the identification of the characteristic flavor compounds in cocoa powder.According to the results,39 compounds which gave contribution to the flavor of cocoa powder were detected,including 7 aldehydes,3 alcohols,3 ketones,8 esters,2 acids,4 pyrazines,2 amines and any other special volatile substances.Among the flavor compounds,three compounds had key odorant(nutty,cocoa flavor),they were 2,5-dimethyl pyrazine,2,3,5-trimethyl pyrazine and 2,3,5,6-tetramethyl pyrazine.

关键词

可可粉/HS-SPME/GC-O/GC-MS/关键风味化合物

Key words

cocoa powder/HS-SPME/GC-O/GC-MS/key odorant compounds

分类

轻工纺织

引用本文复制引用

肖天鹏,郑晓峰,吕吉鸿,郭泽峰,高峰,刘春凤,李崎..顶空固相微萃取结合GC-O与GC-MS技术鉴定可可粉中特征风味化合物[J].食品工业科技,2012,33(18):67-69,72,4.

基金项目

国家“十一五”支撑重点项目资助课题 ()

食品工业科技

OA北大核心CSCDCSTPCD

1002-0306

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